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Photonic integrated circuits Prototyping

Cathodoluminescence and Electron Microscopy Services

Photonic Integrated Circuits

Reference
4.4.5
Lead partner
VU

Technical Scope and Capabilities

This service group provides electron microscopy, cathodoluminescence, EBIC, defect-density evaluation and data-analysis services.

Core Infrastructure / Tools / Equipment

The service uses

  • Attolight Chronos hybrid cathodoluminescence–SEM microscope
  • Digital Surf Attomap software
  • OriginLab Origin software
  • dedicated Python code
  • dedicated C++ code
  • Light Conversion Pharos, Orpheus and Harpia-TG systems for selected services
  • video processing tools for degradation analysis.

Nano-Scale Surface Topography Imaging by SEM

Capabilities and parameters:

  • measurements and basic image post-processing
  • electron acceleration 1–10 keV
  • magnification up to 400k
  • spatial resolution 3 nm
  • image resolution up to 2k × 2k pixels
  • image formats: sur, tif, png, raw
  • probe current 100 fA–100 nA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required.

EBIC Imaging of Electrical Properties

Capabilities and parameters:

  • electron beam induced current imaging
  • measurements and basic image post-processing
  • electron acceleration 1–10 keV
  • spatial resolution diffusion-limited
  • image resolution up to 2k × 2k pixels
  • image formats: sur, tif, png, raw
  • probe current 10–100 nA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required.

Hyperspectral Cathodoluminescence Imaging

Capabilities and parameters:

  • hyperspectral imaging of time-integrated luminescence properties
  • measurements and basic image post-processing
  • electron acceleration 1–10 keV
  • spatial resolution diffusion-limited
  • image resolution up to 512 × 512 pixels
  • file formats for single-wavelength or panchromatic maps: sur, tif, png
  • file formats for hyperspectral maps: sur and video formats
  • probe current 100 fA–100 nA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required
  • sample luminescence efficiency moderate or better
  • sample irradiation resistance moderate or better
  • sample active volume depth 150 nm
  • spectral range 200–900 nm
  • field of view up to 300 micrometres.

Space- and Time-Integrated Cathodoluminescence Spectra

Capabilities and parameters:

  • capture of space- and time-integrated cathodoluminescence spectra
  • measurements and basic data processing
  • electron acceleration 1–10 keV
  • probe current 100 fA–100 nA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required
  • sample luminescence efficiency low or better
  • sample irradiation resistance low or better
  • sample active volume depth 200 nm
  • spectral range 200–900 nm.

Spectra- and Time-Resolved Cathodoluminescence Transients

Capabilities and parameters:

  • capture of spectra- and time-resolved cathodoluminescence transients
  • basic data processing including lifetime extraction
  • electron acceleration 3–10 keV
  • typical spatial resolution 50 nm
  • typical probe current 50 pA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required
  • sample luminescence efficiency low or better for spatially integrated configuration and moderate for spatially resolved configuration
  • sample irradiation resistance low or better for spatially integrated configuration and moderate for spatially resolved configuration
  • sample active volume depth 150 nm
  • spectral range 200–900 nm
  • temporal resolution 20–100 ps
  • pulse repetition rate 2–80 MHz.

Spectro-Spatio-Temporal 4D Imaging of Carrier Dynamics

Capabilities and parameters:

  • spectro-spatio-temporal 4D imaging of carrier dynamics by cathodoluminescence microscopy
  • measurements and basic data processing
  • electron acceleration 3–10 keV
  • typical spatial resolution 50 nm
  • image resolution up to 24 × 24 pixels, upscaled to 96 × 96 pixels
  • typical probe current 50 pA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required
  • sample luminescence efficiency high
  • sample irradiation resistance high
  • sample active volume depth 100 nm
  • spectral range 200–900 nm
  • temporal resolution 20–100 ps
  • pulse repetition rate 2–80 MHz.

Extended Defect Density Evaluation

Capabilities and parameters:

  • evaluation of dislocation and V-pit density
  • cathodoluminescence–electron microscopy
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required
  • sample luminescence efficiency moderate or better
  • sample irradiation resistance moderate or better
  • sample active volume depth 50 nm
  • spectral range 200–900 nm.

Point Defect Density Estimation

Capabilities and parameters:

  • estimation of point defect density using electron-optical approaches
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe and optically clear sample required
  • sample luminescence efficiency moderate or better
  • sample irradiation resistance moderate or better
  • sample active volume depth 50 nm
  • spectral range 260–900 nm.

Material Degradation under Electron Irradiation

Capabilities and parameters:

  • quantification of degradation metrics, including threshold and time
  • electron acceleration 1–10 keV
  • probe current 100 fA–100 nA
  • temperature 10–320 K
  • sample dimensions up to 25 × 25 × 2 mm
  • vacuum-safe sample required
  • sample active volume depth 200 nm
  • spectral range 200–900 nm
  • exposure step of a few seconds.

Bespoke Cathodoluminescence Data Analysis

Capabilities:

  • bespoke analysis of spectro-spatio-temporal cathodoluminescence data
  • Digital Surf Attomap
  • bespoke Python code
  • code licensing under MIT licence.

Carrier Dynamics Characterisation in Wide and Narrow Bandgap Semiconductors